fulltext.study @t Gmail

MCM-41-N-propylsulfamic acid: An efficient catalyst for one-pot synthesis of 1-amidoalkyl-2-naphtols

Paper ID Volume ID Publish Year Pages File Format Full-Text
40006 45842 2014 8 PDF Available
Title
MCM-41-N-propylsulfamic acid: An efficient catalyst for one-pot synthesis of 1-amidoalkyl-2-naphtols
Abstract

•MCM-41-N-propylsulfamic acid was synthesized and characterized.•Synthesis of 1-amidoalkyl-2-naphthols catalyzed by MCM-41-N-propylsulfamic acid.•Used catalyst XRD and IR revealed mesopore channels was stable during reaction.

An efficient, one-pot three-component condensation of aromatic aldehydes, acetamide and 2-naphtol in the presence of catalytic amounts of MCM-41-N-propylsulfamic acid under thermal solvent-free conditions is described for the preparation of 1-amidoalkyl-2-naphtols in good to excellent yields. In this work, MCM-41-N-propylsulfamic acid was prepared by reaction of propylamine functionalized MCM-41 and chlorosulfonic acid and characterized by FTIR, XRD and TGA.

Graphical abstractAn efficient, one-pot three-component condensation of aromatic aldehydes, acetamide and 2-naphtol in the presence of catalytic amounts of MCM-41-N-propylsulfamic acid under thermal solvent-free conditions is described for the preparation of 1-amidoalkyl-2-naphtols.Figure optionsDownload full-size imageDownload high-quality image (116 K)Download as PowerPoint slide

Keywords
1-Amidoalkyl-2-naphtols; MCM-41; MCM-41-N-propylsulfamic acid; Solvent-free; Multicomponent reaction
First Page Preview
MCM-41-N-propylsulfamic acid: An efficient catalyst for one-pot synthesis of 1-amidoalkyl-2-naphtols
Get Full-Text Now
Don't Miss Today's Special Offer
Price was $35.95
You save - $31
Price after discount Only $4.95
100% Money Back Guarantee
Full-text PDF Download
Online Support
Any Questions? feel free to contact us
Publisher
Database: Elsevier - ScienceDirect
Journal: Applied Catalysis A: General - Volume 470, 30 January 2014, Pages 303–310
Authors
, , ,
Subjects
Physical Sciences and Engineering Chemical Engineering Catalysis
Get Full-Text Now
Don't Miss Today's Special Offer
Price was $35.95
You save - $31
Price after discount Only $4.95
100% Money Back Guarantee
Full-text PDF Download
Online Support
Any Questions? feel free to contact us