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An efficient, green and scale-up synthesis of amides from esters and amines catalyzed by Ru-MACHO catalyst under mild conditions

Paper ID Volume ID Publish Year Pages File Format Full-Text
49908 46773 2015 4 PDF Available
Title
An efficient, green and scale-up synthesis of amides from esters and amines catalyzed by Ru-MACHO catalyst under mild conditions
Abstract

•An efficient, green and scale-up synthesis of amides has been developed.•Amides are readily obtained from esters and amines.•Ru-MACHO is used as a readily available catalyst.•Amides are prepared in moderate to excellent yields and on multi-gram scale.

An efficient, green and scale-up synthesis of amides from esters and amines has been developed using Ru-MACHO as a readily available catalyst. A diverse range of amides were obtained in moderate to excellent yields (55–98%). Furthermore, when the scale of the amidation reaction was increased to 240.0 mmol, the desired amide still could be obtained in high yield (48.2 g of N-benzylbenzamide, 95%).

Keywords
WQOOODMDPHYHQS-UHFFFAOYSA-NAmides; Esters; Amines; Ru-MACHO; Green synthesis
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An efficient, green and scale-up synthesis of amides from esters and amines catalyzed by Ru-MACHO catalyst under mild conditions
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Publisher
Database: Elsevier - ScienceDirect
Journal: Catalysis Communications - Volume 58, 5 January 2015, Pages 85–88
Authors
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Subjects
Physical Sciences and Engineering Chemical Engineering Catalysis
Get Full-Text Now
Don't Miss Today's Special Offer
Price was $35.95
You save - $31
Price after discount Only $4.95
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Full-text PDF Download
Online Support
Any Questions? feel free to contact us