fulltext.study @t Gmail

Toward the synthesis of 6-hydroxyquinoline starting from glycerol via improved microwave-assisted modified Skraup reaction

Paper ID Volume ID Publish Year Pages File Format Full-Text
50248 46786 2014 4 PDF Available
Title
Toward the synthesis of 6-hydroxyquinoline starting from glycerol via improved microwave-assisted modified Skraup reaction
Abstract

•Efficient modified Skraup reaction and Bamberger rearrangement•Modified Skraup reaction without As2O5•Synthesis of 6-hydroxyquinoline under microwave irradiation conditions•Synthesis of 6-hydroxyquinoline via a domino reaction

An efficient and modified Skraup reaction and Bamberger rearrangement in neat water were developed using nitrobenzene and an inexpensive, abundant and environmentally-friendly glycerol under microwave irradiation conditions was furnish regioselectively to the 6-hydroxyquinoline. The target compound was obtained in 77% yield via efficient domino reaction with a “one pot eleven steps”.

Graphical abstractFigure optionsDownload full-size imageDownload as PowerPoint slide

Keywords
Glycerol; Skraup; Bamberger; Aqueous catalysis; 6-hydroxyquinoline; Microwaves; Domino reaction
First Page Preview
Toward the synthesis of 6-hydroxyquinoline starting from glycerol via improved microwave-assisted modified Skraup reaction
Get Full-Text Now
Don't Miss Today's Special Offer
Price was $35.95
You save - $31
Price after discount Only $4.95
100% Money Back Guarantee
Full-text PDF Download
Online Support
Any Questions? feel free to contact us
Publisher
Database: Elsevier - ScienceDirect
Journal: Catalysis Communications - Volume 44, 10 January 2014, Pages 15–18
Authors
, , , , , ,
Subjects
Physical Sciences and Engineering Chemical Engineering Catalysis
Get Full-Text Now
Don't Miss Today's Special Offer
Price was $35.95
You save - $31
Price after discount Only $4.95
100% Money Back Guarantee
Full-text PDF Download
Online Support
Any Questions? feel free to contact us