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Consecutive biocatalysis-palladium catalysis II: Synthesis of conduritol-alkyne conjugates ☆

Paper ID Volume ID Publish Year Pages File Format Full-Text
51391 46842 2009 4 PDF Available
Title
Consecutive biocatalysis-palladium catalysis II: Synthesis of conduritol-alkyne conjugates ☆
Abstract

The palladium-catalyzed cross-coupling reaction of potassium alkynyltrifluoroborates with a chemoenzymatically derived deoxyconduritol is described. Six new compounds were synthesized in moderate to good yields. The alkynyl cross-coupling reaction can be effected using 10 mol% of Pd(PPh3)4 as catalyst in toluene–H2O in the presence of Cs2CO3 as the inorganic base.

Keywords
Biocatalysis; Potassium alkynyltrifluoroborates; Cyclitol conjugates
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Consecutive biocatalysis-palladium catalysis II: Synthesis of conduritol-alkyne conjugates ☆
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Publisher
Database: Elsevier - ScienceDirect
Journal: Catalysis Communications - Volume 10, Issue 13, 25 July 2009, Pages 1647–1650
Authors
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Subjects
Physical Sciences and Engineering Chemical Engineering Catalysis
Get Full-Text Now
Don't Miss Today's Special Offer
Price was $35.95
You save - $31
Price after discount Only $4.95
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Full-text PDF Download
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