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Electrochemical synthesis of Pd particles on poly(vinylferrocenium)

Paper ID Volume ID Publish Year Pages File Format Full-Text
51868 46857 2008 4 PDF Available
Title
Electrochemical synthesis of Pd particles on poly(vinylferrocenium)
Abstract

Electrochemical synthesis of Pd particles on poly(vinylferrocenium) (PVF+) support was described. K2PdCl4 was used as the metal particle precursor. Pd particles were incorporated into the polymer matrix electrochemically either by cyclic voltammetric scans (between +1.0 V and −0.8 V vs. SCE) or by reduction at constant potential (at −0.8 V vs. SCE) from aqueous solution of K2PdCl4. Scanning electron microscopy (SEM) studies showed that the Pd particles were well dispersed in the polymer matrix. Experimental parameters such as polymer film thickness, number of cycles during cyclic voltammetric scans in K2PdCl4 and electrolysis time in K2PdCl4 were studied. The Pd/PVF+ system showed catalytic activity towards hydrazine oxidation and appreciable results were obtained when compared with the related studies.

Keywords
Electrocatalysis; Pd particles; Poly(vinylferrocenium); Hydrazine oxidation
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Electrochemical synthesis of Pd particles on poly(vinylferrocenium)
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Publisher
Database: Elsevier - ScienceDirect
Journal: Catalysis Communications - Volume 9, Issue 13, 20 July 2008, Pages 2175–2178
Authors
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Subjects
Physical Sciences and Engineering Chemical Engineering Catalysis
Get Full-Text Now
Don't Miss Today's Special Offer
Price was $35.95
You save - $31
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