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A novel method for the protection of amino alcohols and carbonyl compounds over a heterogeneous, reusable catalyst

Paper ID Volume ID Publish Year Pages File Format Full-Text
52229 46867 2008 5 PDF Available
Title
A novel method for the protection of amino alcohols and carbonyl compounds over a heterogeneous, reusable catalyst
Abstract

A novel application of Al-SBA-15 catalyst in the protection of amino alcohols and carbonyl compounds is reported. N-t-butoxy carbonyl [N(Boc)] amino alcohols were protected using 2,2-dimethoxypropane (DMP) to form acetonides. Acetonide deprotection was also studied using the same catalyst to obtain the parent amino alcohol. Protection of carbonyl compounds was studied using neopentyl glycol, ethylene glycol and propylene glycol as the protecting agents. A series of commercially important molecules such as 2-substituted and 2,2-disubstituted 1,3-benzodioxoles were synthesized by reacting carbonyl compounds with catechol.

Keywords
Protection; Amino alcohol; Acetonide; Acetalization; Benzodioxole
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A novel method for the protection of amino alcohols and carbonyl compounds over a heterogeneous, reusable catalyst
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Publisher
Database: Elsevier - ScienceDirect
Journal: Catalysis Communications - Volume 9, Issue 5, 20 March 2008, Pages 645–649
Authors
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Subjects
Physical Sciences and Engineering Chemical Engineering Catalysis
Get Full-Text Now
Don't Miss Today's Special Offer
Price was $35.95
You save - $31
Price after discount Only $4.95
100% Money Back Guarantee
Full-text PDF Download
Online Support
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