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In situ calcinations of precursors of mesoporous AlPO4 and application of mesoporous Mn–AlPO4

Paper ID Volume ID Publish Year Pages File Format Full-Text
52403 46873 2006 7 PDF Available
Title
In situ calcinations of precursors of mesoporous AlPO4 and application of mesoporous Mn–AlPO4
Abstract

The effects of thermal treatment on as-synthesized AlPO4 were investigated. The in situ X-ray diffraction (XRD), thermogravimetry–differential thermal analysis (TGA–DTA), in situ Fourier transform infrared (FTIR) spectroscopy, scanning electron microscopy (SEM), and 27Al, 31P MAS-NMR were utilized to characterize physical properties of synthesized AlPO4, including phase, crystalline, structure, and morphology. Results showed that Mn substituted a portion of Al in the frameworks of mesoporous AlPO4. When being applied to tert-butylation of m-cresol with tert-butyl alcohol, Mn–AlPO4 achieved a tert-butyl alcohol conversion of 20.2 wt% after being circulated for 5 times.

Keywords
In situ; Precursor; Calcinations; Mesoporous AlPO4
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In situ calcinations of precursors of mesoporous AlPO4 and application of mesoporous Mn–AlPO4
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Publisher
Database: Elsevier - ScienceDirect
Journal: Catalysis Communications - Volume 7, Issue 11, November 2006, Pages 848–854
Authors
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Subjects
Physical Sciences and Engineering Chemical Engineering Catalysis
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Price was $35.95
You save - $31
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