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Synthesis, characterization and catalytic activity of meso-niobium phosphate in the oxidation of benzyl alcohols

Paper ID Volume ID Publish Year Pages File Format Full-Text
55163 47042 2012 6 PDF Available
Title
Synthesis, characterization and catalytic activity of meso-niobium phosphate in the oxidation of benzyl alcohols
Abstract

In this work mesoporous niobium phosphate was synthesized hydrothermally by using SDS as the structure directing agent. The catalysts were characterized by N2 adsorption, DRX, 31P MAS NMR and FTIR. The activity of commercial and synthesized niobium phosphate catalysts were evaluated through the oxidation of benzyl alcohol and 1-phenylethanol in the presence of hydrogen peroxide. Good conversion and selectivity to oxidation products were obtained in mild conditions.

Graphical abstractFigure optionsDownload full-size imageDownload high-quality image (61 K)Download as PowerPoint slideHighlights► Mesoporous niobium phosphate was synthesized by using SDS as structure directing agent and the surface area was 263 m2 g−1. ► Mesoporous niobium phosphate improved the conversion of benzyl alcohols in the oxidation reaction with hydrogen peroxide. ► Better conversion and selectivity were obtained for the oxidation of 1-phenylethanol.

Keywords
Oxidation; Niobium phosphate; Niobia; Mesoporous materials; Benzyl alcohol
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Synthesis, characterization and catalytic activity of meso-niobium phosphate in the oxidation of benzyl alcohols
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Publisher
Database: Elsevier - ScienceDirect
Journal: Catalysis Today - Volume 192, Issue 1, 30 September 2012, Pages 117–122
Authors
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Subjects
Physical Sciences and Engineering Chemical Engineering Catalysis
Get Full-Text Now
Don't Miss Today's Special Offer
Price was $35.95
You save - $31
Price after discount Only $4.95
100% Money Back Guarantee
Full-text PDF Download
Online Support
Any Questions? feel free to contact us